A review of green solvent extraction techniques and their use in antibiotic residue analysis

Khataei, Mohammad Mahdi; Epi, Shazalatun Binte Huda; Lood, Rolf; Spégel, SpegelPeter; Yamini, Yadollah; Turner, Charlotta

doi:10.1016/j.jpba.2021.114487

Cited by 34 publications

(11 citation statements)

References 165 publications

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“…Different extraction efficiencies for different classes of antibiotics were reported. Dispersive solid phase extraction (dSPE) cleanup was proposed to reduce the matrix effects but resulted in lower recoveries for some classes of antibiotics, especially for tetracycline compounds [39,40].…”

Section: Optimization Of Extraction Of Antibioticsmentioning

confidence: 99%

Determination of Multi-Class Antibiotics Residues in Farmed Fish and Shrimp from Sri Lanka by Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry (UPLC-MS/MS)

Jayasinghe

Szpunar

Łobiński

et al. 2023

Fishes

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Antibiotics have been used to control the aquatic environment in both therapeutic and prophylactic ways. Antibiotics are particularly difficult to extract due to their strong interactions with biological matrices. In this study, UPLC-MS/MS method was developed and validated for quantitative confirmatory analysis of multi-class antibiotics residues in fish and shrimp. Fourteen antibiotics belonging to sulphonamides, β-lactams, quinolones, sulfones and macrolides were determined within one chromatographic run. The samples were suspended in 0.1 M HCl, and the analytes were extracted into ethyl acetate. The extracts were defatted with cyclohexane. The limits of quantification (LOQ) ranged from 0.24 to 1.32 µg kg−1 for fish and 0.42–1.62 µg kg−1 for shrimp samples. The recoveries ranged from 75 to 105%. The method was applied to the analysis of farmed freshwater Tilapia fish (Oreochromis niloticus) and shrimp (Penaeus monodon) collected in Sri Lanka. Sulfacetamide (4.31 ± 0.70 µg kg−1) and sulfamethoxypyridazine (0.75 ± 0.15 µg kg−1) were detected in the fish, and sulfapyridine (0.21–0.56 µg kg−1) and sulfadoxine (0.35–1.44 µg kg−1) were detected in the shrimp samples. The concentrations complied with the EU regulation limits for veterinary drug residues in seafood and did not pose a risk in terms of food safety.

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Section: Optimization Of Extraction Of Antibioticsmentioning

confidence: 99%

Determination of Multi-Class Antibiotics Residues in Farmed Fish and Shrimp from Sri Lanka by Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry (UPLC-MS/MS)

Jayasinghe

Szpunar

Łobiński

et al. 2023

Fishes

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“…Several modi-cations have been suggested by many researchers, such as changing solvents due to their toxic nature. 100,101 In response to health and environmental concerns, green solvents like supercritical uid (CO 2 ), plant-derived terpenes and ionic liquids are emerging. However, supercritical uid extraction is not commonly used for FOG analysis, and further research is needed to evaluate its feasibility and performance compared to other extraction methods.…”

Section: Future Perspectivementioning

confidence: 99%

Component analysis of fat, oil and grease in wastewater: challenges and opportunities

Mohana,

Roddick,

Maniam

et al. 2023

Anal. Methods

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“…19 Therefore, sample pretreatment was required before further analysis. Some sample preparation methods have been used to extract the target from food matrices such as liquid-liquid extraction (LLE), 20,21 QuEChERS (quick, easy, cheap, effective, rugged, safe), 22 solid phase extraction (SPE) 23,24 and solid-phase microextraction (SPME). 25 Among these methods, SPE typically stands out due to several advantages, including a short extraction time, cost-effectiveness, less use of organic solvents, simple and quick operation, and good reproducibility.…”

Section: Introductionmentioning

confidence: 99%

Design of a novel green bio-based organic–inorganic hybrid material for cost-effective and sustainable monitoring of antibiotic residues

Qin,

Song,

et al. 2024

Green Chem.

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A review of green solvent extraction techniques and their use in antibiotic residue analysis

Cited by 34 publications

References 165 publications

Determination of Multi-Class Antibiotics Residues in Farmed Fish and Shrimp from Sri Lanka by Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry (UPLC-MS/MS)

Determination of Multi-Class Antibiotics Residues in Farmed Fish and Shrimp from Sri Lanka by Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry (UPLC-MS/MS)

Component analysis of fat, oil and grease in wastewater: challenges and opportunities

Design of a novel green bio-based organic–inorganic hybrid material for cost-effective and sustainable monitoring of antibiotic residues

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