The mechanical properties of novel alloys with two-phase -TiAl + -Nb2Al microstructures were evaluated under compression at room temperature. Microstructures of varying scales were developed through solutionizing and aging heat treatments and the volume fraction of phases were varied with changes in composition. Ultra-fine, aged + microstructures were achieved for the alloys which affectively retained high volume fractions of the parent -phase upon quenching from the solutionizing temperature. The yield strength and compressive strain to failure of these alloys show a strong dependence on the relative scale and volume fraction of phases. Surprisingly, the hard brittle phase particles were not found to control fracture in the refined microstructures.