Experimental replication of stone tools is an important method for understanding the context and production of prehistoric technologies. In scientific undertakings, experimental control is a valuable and necessary means of ensuring that confounding variables are not influencing the outcomes of the study. One way that researchers can exert control in knapping experiments is to standardize the type, form, and size of raw materials that are provided to the knappers. Though measures to standardize materials are already part of archaeological practice, specific protocols, let alone comparisons between standardization techniques, are rarely openly reported. Consequently, independent laboratories often repeat the same trial-and-error process for selecting the ‘right’ material for testing. We investigate a variety of techniques and raw materials (e.g., hand-knapped flint, machine-cut basalt, manufactured glass, and porcelain). Each material was evaluated for their validity, reliability, and ease of standardization. Here, we have outlined the raw material tests we performed, providing information on the individual approaches, as well as comparisons between the techniques and materials according to both validity and reliability, along with their costs and our own recommendations. This text is intended as a serviceable guide on raw material standardization for knapping experiments, including previously pursued avenues and means that are as-of-yet undescribed in the experimental archaeology literature. We include additional considerations for techniques that were not included in this study or which are presently not widely available and/or affordable. Future potential in this field would benefit from advances in the relevant technologies and in methodological approaches.