1985
DOI: 10.1080/00103628509367628
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A wet oxidation procedure suitable for total nitrogen and phosphorus in soil

Abstract: A wet oxidation digestion previously developed for plant material has now been evaluated for a range of British soil types. The traditional Kjeldahl procedure using sulphuric acid, salt and catalyst was modified to include hydrogen peroxide as an additional oxidant. The method is suitable for estimating both nitrogen and phosphorus in soil and overcomes the need for separate digestion procedures for these elements. It compared favourably with a normal Kjeldahl method for nitrogen and with a mixed acid oxidatio… Show more

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Cited by 44 publications
(16 citation statements)
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“…Total soil C and total N concentrations were measured by dry combustion (Leco CNS-1000, Leco Corp., St-Joseph, MI). Total soil P content was determined by wet oxidation as described by Rowland and Grimshaw (1985).…”
Section: Methodsmentioning
confidence: 99%
“…Total soil C and total N concentrations were measured by dry combustion (Leco CNS-1000, Leco Corp., St-Joseph, MI). Total soil P content was determined by wet oxidation as described by Rowland and Grimshaw (1985).…”
Section: Methodsmentioning
confidence: 99%
“…Water content for the samples was determined by preand post-weighing of well-mixed subsamples dried at 60°C for 24 h. Organic content was determined as losson-ignition (LOI) by ashing at 550°C for 3 h. Total phosphorus concentration was determined using the molybdenum blue reaction on a SEAL AQ2 auto analyser (Seal Analytical Ltd., Fareham, Hampshire, U.K.) following a 2-h hot sulphuric acid-hydrogen peroxide digestion (Rowland & Grimshaw, 1985). Particle size analysis was carried out on a Malvern Mastersizer 2000 (Malvern Instruments Limited, Malvern, Worcestershire, U.K.) after heating for 3 h in hydrogen peroxide to remove organic material and passing through a 2-mm sieve.…”
Section: Field and Laboratory Methodsmentioning
confidence: 99%
“…Organic content was determined as loss-on-ignition (LOI) then by ashing at 550˚C for three hours. Total phosphorus concentration was determined using the molybdenum blue reaction on a SEAL AQ2 auto analyser (Seal Analytical Ltd., Fareham, Hampshire, UK) following a two hour hot sulphuric acid-hydrogen peroxide digestion (Rowland & Grimshaw, 1985).…”
Section: Field and Laboratory Methodsmentioning
confidence: 99%
“…Both total N and total P were calculated based on the oven-dry (105°C [221°F]) weight of the soil. Soil total N was determined by micro-Kjeldahl digestion, and soil total P was determined by the wet oxidation procedure described by Rowland and Grimshaw (1985).…”
mentioning
confidence: 99%