2021
DOI: 10.26434/chemrxiv-2021-r9c0c
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Acceleration of alkyne metathesis in multicomponent catalytic systems by use of alternative Mo(0) sources under optimised conditions

Abstract: Abstract. Alkyne metathesis in multicomponent catalytic systems, although subject to changes, is still a domain of molybdenum hexacarbonyl as a source of Mo(0). Our findings show that this coordination compound is relatively inert under metathesis conditions, which results in noticeably long induction of catalytic activity, and the kinetics of this transformation can greatly benefit from switching to more labile Mo(0) complexes. Several easily obtainable ones had been tested and [Mo(CO)3(py)3] has been chosen … Show more

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