“…Volatile compounds present in FPS, prepared using various pretreatment processes, were identied utilizing SPME coupled with GC-MS, and quantied relative to the internal standard 1,2-dichlorobenzene employing a semi-quantitative approach. Table S1 (ESI) † illustrates the identication of a total of 115 volatile compounds, categorized into 12 main types, including alkenes (26), ketones (14), acids (2), alcohols (11), aldehydes (23), phenols (3), ethers (2), esters (12), hydrocarbons (8), pyrazines and pyrroles (5), furans (2), and others (7), where (n) represents the number of different volatile compounds identi-ed. The number of volatiles detected in samples FPS1-FPS9 ranged from 92 to 102.…”