1994
DOI: 10.1136/gut.35.11.1653
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Addition of dimethylsulphoxide to methyl-tert-butyl ether and ethyl propionate increases cholesterol dissolving capacity and cholesterol gall stone dissolution in vitro.

Abstract: There is a discrepancy between in vitro cholesterol dissolving efficacy of methyltert-butyl ether (MTBE)

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“…The obtained “raw complex” is a visibly “wet” dark red powder because it contains an excessive, nonbound liquid DESO. In an independent test, DESO was found to be well miscible with MTBE, consistently with good solubility 34 of similar compound DMSO in MTBE. In step 1 of purification, the “raw complex” in a 5 mL vial was mixed with 5 mL MTBE as “purification solvent,” the vial was closed, the obtained suspension was stirred for 30 min, stirring was stopped, the powder was allowed to settle, and clear supernatant was removed.…”
Section: Methodsmentioning
confidence: 59%
“…The obtained “raw complex” is a visibly “wet” dark red powder because it contains an excessive, nonbound liquid DESO. In an independent test, DESO was found to be well miscible with MTBE, consistently with good solubility 34 of similar compound DMSO in MTBE. In step 1 of purification, the “raw complex” in a 5 mL vial was mixed with 5 mL MTBE as “purification solvent,” the vial was closed, the obtained suspension was stirred for 30 min, stirring was stopped, the powder was allowed to settle, and clear supernatant was removed.…”
Section: Methodsmentioning
confidence: 59%