Additive Manufacturing of Ceramic Products Based on Millimeter-Wave Heating

Abstract

Additive manufacturing of ceramic articles making use of concentrated energy flows attracts the research interest worldwide. While the application of laser beams faces serious problems associated with high temperature of sintering and low thermal conductivity of ceramics, layer-by-layer sintering by focused millimeter-wave radiation appears to be a promising method of additive manufacturing. This paper describes the studies of fast millimeter-wave sintering of yttria-stabilized zirconia and hydroxyapatite ceramics. Coefficients of the millimeter-wave absorption have been determined in broad frequency and temperature ranges. Rapid sintering of compacted ceramics samples was accomplished using volumetric microwave heating in a work chamber of a 24 GHz / 5 kW gyrotron system. In addition, using a 263 GHz / 1 kW cwgyrotron millimeter-wave source and a purposely designed electrodynamic focusing structure, radiation intensities of up to 20 kW/cm2could be achieved, which was sufficient for fast localized heating of ceramic layers to the solidification temperature. The results of a study of the microstructure and mechanical properties of the sintered ceramics are presented.