Adsorption of chromium(III), mercury(II) and lead(II) ions onto 4-aminoantipyrine immobilized bentonite

Wang, Qihui; Chang, Xijun; Li, Dandan; Hu, Zheng; Li, Ruijun; He, Qun

doi:10.1016/j.jhazmat.2010.11.107

Cited by 84 publications

(24 citation statements)

References 31 publications

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“…The supernatants were used to estimate residual metal concentration by ICP-OES. Biosorbent capacity is the most important factor, for it limits how much biosorbent is required to quantitatively remove a certain amount of metal ions from aqueous solutions (Wang et al 2011). Thus, the maximum biosorption capacity of B. subtilis immobilized on Amberlite XAD-16 was determined as 12.4 and 10.3 mg/g for Cu 2C and Ni 2C , respectively.…”

Section: Analytical Features Of Spe Methodsmentioning

confidence: 99%

Preconcentration withBacillus subtilis–Immobilized Amberlite XAD-16: Determination of Cu²⁺and Ni²⁺in River, Soil, and Vegetable Samples

Okumuş

Özdemir

Kılınç

et al. 2015

Bioremediation Journal

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Solid-phase extraction (SPE) method was developed for the preconcentration of Cu 2C and Ni 2C before their determination by inductively coupled plasma optical emission spectrometry (ICP-OES). Bacillus subtilisimmobilized Amberlite XAD-16 was used as biosorbent. Effects of critical parameters such as pH, flow rate of samples, amount of Amberlite XAD-16 and biosorbent, sample volume, eluent type, and volume and concentration of eluent on column preconcentration of Cu 2C and Ni 2C were optimized. Applicability of the method was validated through the analysis of the certified reference tea sample (NCS ZC73014). Sensitivity of ICP-OES was improved by 36.4-fold for Cu 2C and 38.0-fold for Ni 2C by SPE-ICP-OES method. Limit of quantitation (LOQ) was found to be 0.7 and 1.1 ng/ml for Cu 2C and Ni 2C , respectively. Concentrations of Cu 2C and Ni 2C were determined by ICP-OES after application of developed method. Relative standard deviations (RSDs) were lower than 4.9% for Cu 2C and 7.9% for Ni 2C . The Tigris River that irrigates a large agricultural part of Southeast Turkey is polluted by domestic and industrial wastes. Concentrations of Cu 2C and Ni 2C were determined in water, soil, and some edible vegetables as a biomonitor for heavy metal pollution.

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Section: Analytical Features Of Spe Methodsmentioning

confidence: 99%

Preconcentration withBacillus subtilis–Immobilized Amberlite XAD-16: Determination of Cu²⁺and Ni²⁺in River, Soil, and Vegetable Samples

Okumuş

Özdemir

Kılınç

et al. 2015

Bioremediation Journal

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“…It is important to determine how much biosorbent is required to quantitatively remove a specific amount of metal ions from a solution [53]. To investigate this, 0.25 g C. versicolor immobilised on 1.0 g of Amberlite XAD-4 was packed in a column.…”

Section: Analytical Characteristics Of the Methodsmentioning

confidence: 99%

Selective preconcentration of Lanthanum(III) byCoriolus versicolorimmobilised on Amberlite XAD-4 and its determination by ICP-OES

Özdemir

Okumuş

Dündar

et al. 2013

International Journal of Environmental Analytical Chemistry

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“…The flow rates of metal ion solution in biosorption column are important parameters to control the biosorption times and the biosorption result analysis because the retention elements on the biosorbent depend on the flow rates of the sample solution (Wang et al 2011). From that point of view, the effect of the flow rate of sample solution on the recovery of Cu(II) and Pb(II) was investigated under optimum conditions.…”

Section: Effect Of Flow Ratementioning

confidence: 99%

Anoxybacillussp. SO B1–Immobilized Amberlite XAD-16 for Solid-Phase Preconcentration of Cu(II) and Pb(II) and Their Determinations by Flame Atomic Absorption Spectrometry

Oral

Özdemir

Dolak

et al. 2015

Bioremediation Journal

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A new method for the determination of Cu(II) and Pb(II) by flame atomic absorption spectrometry (FAAS) after preconcentrating on a column containing Anoxybacillus sp. SO B1-immobilized Amberlite XAD-16 was developed. The functional groups of Anoxybacillus sp. SO B1 immobilized on Amberlite XAD-16 were characterized in KBr tablets by Fourier transform infrared (FT-IR) spectrometry. Various parameters such as pH, amount of the adsorbent, eluent type and volume, and flow rate of the sample solution were studied. The optimum pH values of quantitative sorption for Cu(II) and Pb(II) were found to be pH 7.0 and 5.0 and Cu(II) and Pb(II) ions could be quantitatively eluted with 5.0 ml of 1.0 mol L ¡1 HCI and 10.0 ml of 0.25 mol L ¡1 HNO 3 , respectively. Recoveries of Cu(II) and Pb(II) were found to be 100.9 § 1.57% and 100.3 § 0.49% (N D 5), the limits of detection of Cu(II) and Pb(II) in the determination by FAAS (3 s, N D 10) were found to be 0.8 and 1.6 mg L ¡1 , respectively. The proposed enrichment method was applied for metal ion determination from water samples such as two parts of Tigris River water in Diyarbakır and Elazı g, Lake of Hazar in Elazı g, and tap water in Diyarbakır. Furthermore, the accuracy of the proposed method was verified by studying the analytical recovery and by analyzing certified reference material (NCS-DC 73350 leaves of poplar).

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Adsorption of chromium(III), mercury(II) and lead(II) ions onto 4-aminoantipyrine immobilized bentonite

Cited by 84 publications

References 31 publications

Preconcentration withBacillus subtilis–Immobilized Amberlite XAD-16: Determination of Cu²⁺and Ni²⁺in River, Soil, and Vegetable Samples

Preconcentration withBacillus subtilis–Immobilized Amberlite XAD-16: Determination of Cu²⁺and Ni²⁺in River, Soil, and Vegetable Samples

Selective preconcentration of Lanthanum(III) byCoriolus versicolorimmobilised on Amberlite XAD-4 and its determination by ICP-OES

Anoxybacillussp. SO B1–Immobilized Amberlite XAD-16 for Solid-Phase Preconcentration of Cu(II) and Pb(II) and Their Determinations by Flame Atomic Absorption Spectrometry

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Adsorption of chromium(III), mercury(II) and lead(II) ions onto 4-aminoantipyrine immobilized bentonite

Cited by 84 publications

References 31 publications

Preconcentration withBacillus subtilis–Immobilized Amberlite XAD-16: Determination of Cu2+and Ni2+in River, Soil, and Vegetable Samples

Preconcentration withBacillus subtilis–Immobilized Amberlite XAD-16: Determination of Cu2+and Ni2+in River, Soil, and Vegetable Samples

Selective preconcentration of Lanthanum(III) byCoriolus versicolorimmobilised on Amberlite XAD-4 and its determination by ICP-OES

Anoxybacillussp. SO B1–Immobilized Amberlite XAD-16 for Solid-Phase Preconcentration of Cu(II) and Pb(II) and Their Determinations by Flame Atomic Absorption Spectrometry

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Preconcentration withBacillus subtilis–Immobilized Amberlite XAD-16: Determination of Cu²⁺and Ni²⁺in River, Soil, and Vegetable Samples

Preconcentration withBacillus subtilis–Immobilized Amberlite XAD-16: Determination of Cu²⁺and Ni²⁺in River, Soil, and Vegetable Samples