An Alternative Method for the Synthesis of S-Methylmethanethiosulfonate

Abstract

Attempts will be made to explore the potential of S-Methylmethanethiosulfonate towards various organophosphorus compounds. ExperimentalCaution: This sulfenate should be handled carefully as it possesses a pungent smell and may cause vomiting and headache). Synthesis of Compound (2):A mixture of DMSO (23.4 g, 0.30 mol) and TiCl 4 (0.190 g, 0.009 mol