“…Compared to the individual FeCo-S, the positions of the Fe 2p 3/2 and Fe 2p 1/2 peaks have shifted to lower energy by 0.7 and 2.7 eV, respectively. It is indicate that the Co 2p spectrum of FeCo-S-Ni 2 P/NF exhibits six typical peaks at 774.8, 779.8, 785.4, 792.4, 795.7, and 800.2 eV, corresponding to Co 3+ , Co 2+ , satellite peak, Co 3+ , Co 2+ , and satellite peak (Figure c). , Compared to the individual FeCo-S, the positions of the two Co 2+ peaks have shifted to lower energy by 1.4 and 2.0 eV. Notably, characteristic peaks of FeP and CoP were not detected, indicating that the composition of FeCo-S coated on NF did not change during the phosphorization process, further confirming the successful synthesis of the FeCo-S/Ni 2 P/NF heterostructure.…”