1968
DOI: 10.1088/0022-3735/1/10/414
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An electrolytic grinding machine

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Cited by 3 publications
(2 citation statements)
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“…133,143,145,146 Normally, the preparation of the thin TEM specimen is composed of three steps, (a) obtaining a sample piece less than 2 mm thick, (b) mechanically thinning the sample down to about 0.2 mm and (c) further decreasing the sample thickness down to nanometre range so that sufficient electron beam penetration can occur. 147 The key factors of electropolishing, including voltage, current density, temperature, electropolishing duration and convective flow rate need to be carefully optimised in order for one to obtain an ideal TEM sample for reproducible observation. Necip 148 prepared high quality pure aluminium TEM samples through a double-jet electropolishing technique.…”
Section: Electron Microscopementioning
confidence: 99%
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“…133,143,145,146 Normally, the preparation of the thin TEM specimen is composed of three steps, (a) obtaining a sample piece less than 2 mm thick, (b) mechanically thinning the sample down to about 0.2 mm and (c) further decreasing the sample thickness down to nanometre range so that sufficient electron beam penetration can occur. 147 The key factors of electropolishing, including voltage, current density, temperature, electropolishing duration and convective flow rate need to be carefully optimised in order for one to obtain an ideal TEM sample for reproducible observation. Necip 148 prepared high quality pure aluminium TEM samples through a double-jet electropolishing technique.…”
Section: Electron Microscopementioning
confidence: 99%
“…133,143,145,146 Normally, the preparation of the thin TEM specimen is composed of three steps, (a) obtaining a sample piece less than 2 mm thick, (b) mechanically thinning the sample down to about 0.2 mm and (c) further decreasing the sample thickness down to nanometre range so that sufficient electron beam penetration can occur. 147…”
Section: Electropolishing Evaluation With Microscopementioning
confidence: 99%