An improved synthesis of catechol‐U‐<sup>14</sup>C

Acetylene[14C2] is shown to be a useful starting material for the synthesis of a number of 14C‐labeled intermediates and small molecules. Its facile preparation from inexpensive barium carbonate[14C] and the range of transformations it undergoes allow the efficient syntheses of 2‐propyn‐[2,3‐14C2]‐1‐ol, 2‐propen[2,3‐14C2]‐1‐ol, 2‐propen[G‐14C]yl‐isothiocyanate, 2‐butanone[1,2‐14C2], furan[3,4‐14C2], p‐dioxane[U‐14C], and various other intermediates.

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Efficient syntheses of a variety of labeled compounds from acetylene[¹⁴C₂]

Heys

Rotert

Hicks

et al. 1983

Labelled Comp Radiopharmac

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Preparation of carbon‐14 and tritium labelled 2‐sec‐butylphenyl n‐methyl carbamate (BPMC)

Rutkai

Kling

Bursics

et al. 1988

Labelled Comp Radiopharmac

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Preparative separation of polar unstable compounds (catecholamines) from a synthetic mixture by high-speed counter-current chromatography

Weisz

Markey

Ito

1986

Journal of Chromatography B: Biomedical Sciences and Applicatio

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An improved synthesis of catechol‐U‐¹⁴C

Abstract: SUMMARYThe high yield, four-step synthesis of ~a t e c h o l -U -~~C from benzeneIntermediates in the preparation include phenol-U-14C U-14C is described. and g-meth~xyphenol-U-~~C [g~aiacol-(phenyl-U-~~C)].

Cited by 3 publications

References 9 publications

Efficient syntheses of a variety of labeled compounds from acetylene[¹⁴C₂]

Efficient syntheses of a variety of labeled compounds from acetylene[¹⁴C₂]

Preparation of carbon‐14 and tritium labelled 2‐sec‐butylphenyl n‐methyl carbamate (BPMC)

Preparative separation of polar unstable compounds (catecholamines) from a synthetic mixture by high-speed counter-current chromatography

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An improved synthesis of catechol‐U‐14C

Abstract: SUMMARYThe high yield, four-step synthesis of ~a t e c h o l -U -~~C from benzeneIntermediates in the preparation include phenol-U-14C U-14C is described. and g-meth~xyphenol-U-~~C [g~aiacol-(phenyl-U-~~C)].

Cited by 3 publications

References 9 publications

Efficient syntheses of a variety of labeled compounds from acetylene[14C2]

Efficient syntheses of a variety of labeled compounds from acetylene[14C2]

Preparation of carbon‐14 and tritium labelled 2‐sec‐butylphenyl n‐methyl carbamate (BPMC)

Preparative separation of polar unstable compounds (catecholamines) from a synthetic mixture by high-speed counter-current chromatography

Contact Info

Product

Resources

About

An improved synthesis of catechol‐U‐¹⁴C

Efficient syntheses of a variety of labeled compounds from acetylene[¹⁴C₂]

Efficient syntheses of a variety of labeled compounds from acetylene[¹⁴C₂]