1971
DOI: 10.1007/bf00372231
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An interlaboratory comparison of piston-cylinder pressure calibration using the albite-breakdown reaction

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Cited by 218 publications
(59 citation statements)
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“…Such a large assembly minimises frictional loss and shear stress at lower pressures (Johannes et al 1971). A double capsule technique was used to buffer fO 2 .…”
Section: Experimental Methodsmentioning
confidence: 99%
“…Such a large assembly minimises frictional loss and shear stress at lower pressures (Johannes et al 1971). A double capsule technique was used to buffer fO 2 .…”
Section: Experimental Methodsmentioning
confidence: 99%
“…The pressure medium for all experiments consisted of a CaF 2 sleeve. Pressure was applied using the cold piston-in technique (Johannes et al, 1971). The friction correction for the assemblies was calibrated against the Ca-Tschermakite breakdown reaction at 1.2 to 1.4 GPa and 1300 °C (Hays, 1966) and determined to be less than the pressure uncertainty associated with the experiments, so that no correction has been applied to the reported pressure.…”
Section: Experimental Methodsmentioning
confidence: 99%
“…Using a Johannes-type piston cylinder, pressure can be directly measured by a load cell built into the frame (Johannes 1973) and is considered to be accurate to ±0.043 GPa (Molina andPoli 2000Schmidt 1992). Calibration was performed against the reaction albite = jadeite + quartz (Johannes et al 1971) and no friction was observed compared to values obtained form load cell as a result of the large volume NaCl salt sleeve used. During each run, pressure was first increased to 1.5 GPa and then the assembly was isobarically heated at a constant heating rate (≈50 °C/min) until the target temperature was reached.…”
Section: Piston-cylinder Experimentsmentioning
confidence: 99%