Abstract. We shall prove a new generalization of Vosper critical pair theorem to finite Abelian groups. We next apply this new tool to the theory of (k, l)-free sets in finite Abelian groups. In particular, in most cases, we describe the structure of maximal (k, l)-free sets and determine the maximal cardinality of such a set. This result allows us for instance to give precisions on an old result of Yap: we are able to describe completely the maximal sum-free sets with cardinality at least one third of that of the ambient group.