2024
DOI: 10.20944/preprints202401.0402.v1
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An <em>In-Situ</em> Mössbauer Study of the High-Temperature Behavior of Siderite under Reduction Conditions

Mariola Kądziołka-Gaweł,
Zdzisław Adamczyk,
Mateusz Dulski
et al.

Abstract: The thermal decomposition of siderite and its decomposition products in a vacuum atmosphere was investigated for the first time using in situ high-temperature transmission Mössbauer spectroscopy. These measurements were supported by X-ray diffraction, Raman spectroscopy, X-ray fluorescence, and magnetic measurements. In situ Mössbauer spectra were collected from room temperature (RT) to 750 oC with a temperature step of 50 oC. After that, the sample was cooled down to RT with step 100 oC. Raw siderite samples … Show more

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