2020
DOI: 10.1016/j.mex.2020.101010
|View full text |Cite
|
Sign up to set email alerts
|

Analysis of pharmaceuticals in fish using ultrasound extraction and dispersive spe clean-up on que Z-Sep/C18 followed by LC-QToF-MS detection

Abstract: The presence of pharmaceutically active compounds (PhACs) in aquatic biota has been received much less attention than their presence in surface or waste water, and it was not until the mid-2000s, this gap started to be addressed. Here, we present SQUEEZe ( S olid-li Q uid U ltrasound E xtraction with Qu E Z -S e p/C18 as dispersive clean-up): a fas… Show more

Help me understand this report

Search citation statements

Order By: Relevance

Paper Sections

Select...
1
1

Citation Types

0
3
0

Year Published

2021
2021
2023
2023

Publication Types

Select...
5

Relationship

2
3

Authors

Journals

citations
Cited by 9 publications
(3 citation statements)
references
References 32 publications
0
3
0
Order By: Relevance
“…The use of isotopically labelled Internal Standards (I.S.) serves for compensate the matrix effect (signal enhancement/suppression) but also improves accuracy and precision [25] . A matrix-matched calibration curve (CC) was elaborated using blank radishes and spiking them using at least eight different curve points, ranging from 0.05 to 300 ng mL −1 in dry weight radish.…”
Section: Methods Validationmentioning
confidence: 99%
“…The use of isotopically labelled Internal Standards (I.S.) serves for compensate the matrix effect (signal enhancement/suppression) but also improves accuracy and precision [25] . A matrix-matched calibration curve (CC) was elaborated using blank radishes and spiking them using at least eight different curve points, ranging from 0.05 to 300 ng mL −1 in dry weight radish.…”
Section: Methods Validationmentioning
confidence: 99%
“…Due to the low expected levels of CECs and the complexity of the matrix, sensitive and robust analytical methods are essential. Ultrasound-assisted solvent extraction (UAE) is one of the most common extraction methods for CECs in aquatic biota [ 9 , 12 , 21 32 ]. Extraction of complex biological matrices typically features a clean-up step to ensure removal of co-extracted matrix components that otherwise may interfere in the quantification.…”
Section: Introductionmentioning
confidence: 99%
“…Journal of Chromatography A, 461009 (2020) [1] . Peña-Herrera J.M., Montemurro N., Barceló D., Pérez S. Analysis of pharmaceuticals in fish using ultrasound extraction and dispersive SPE clean-up on QuE Z-Sep/C18 followed by LC-QToF-MS detection [2] . Aceña, J., Pérez, S., Eichhorn, P. Solé, M., Barceló, D.1.…”
mentioning
confidence: 99%