CCDC no.: 1441404The crystal structure is shown in the gure, Tables 1-3 contain details of the measurement method and a list of the atoms including atomic coordinates and displacement parameters.
Source of materialA mixture of Cu(OAc) 2 ·H 2 O (0.1 mmol, 199 mg), THF (10 mL), 4-(3-(pyridin-3-yl)-1H-1,2,4-triazol-5-yl)benzoic acid (0.3 mmol, 266 mg) was dissolved in 8 mL H 2 O. Then the solution was heated in a 23 mL Te on-lined autoclave under autogenous pressure at 393 K for ve days. After cooling to room temperature crystals formed. The red crystals suitable for X-ray di raction analysis were collected.
Experimental detailsAt the pyridine ring, the hydrogen atoms were assigned with U iso (H) = 1.2 Ueq(C), and included in the nal re nement by