The machining of extremely hard material in conventional machining requires
high energy. Therefore stress-free, burr-free, and high-accuracy machining
technique like Electro Chemical Micro Machining (ECMM) with extra features
is recommended. To improve efficiency, various electrolytes such as Magnet
Associated Electrolytes (MGAE), Metal Particle Mixed Electrolytes (MPME),
and Carbon Pellets Mixed Electrolytes (CPME) are employed. The micro-holes
were drilled over the work material MONEL 400 alloy. The parameters for the
studies are electrolyte type, concentration (g/l), machining voltage (V),
and duty cycle (%). The responses of ECMM are estimated through material
removal rate (MRR) in ?m/sec and overcut in ?m. The results are optimized
using Multi-objective optimization based on ratio analysis (MOORA) and
VlseKriterijumska Optimizacija I Kompromisno Resenje (VIKOR). Both
techniques produce the same optimal parameter, 18th experiment CPME, 50%
duty cycle, 11 V machining voltage, and 28 g/l electrolyte concentration. It
is the best optimal parameter solution for machining. According to the ANOVA
table of both, the type of electrolyte plays a 62.6 % and 60.37%
contribution, respectively, to machining performance. Furthermore, the
scanning electron microscope (SEM) image analysis perused on the micro holes
to extend the effect of different electrolytes on machining surfaces.