A New Schiff based resin Poly-methylene bis (2-methyoxy-1-napthaldehyde) 1, 2-propylenediimine (PMBMNPn) was synthesized by reacting with Formaldehyde (HCHO). The synthesized resin was categorized through elemental micro-analysis and Fourier transformation. The infrared, ultraviolet and visible spectroscopic analysis TGA/DTA and Viscometric studies were also carried out. The results of Carbon-Hydrogen-Nitrogen (CHN) Analysis were in good agreement with the considered values and reinforced the formation of the prepared resin. The resin indicated more strong absorption around 16 to 35 cm-1 of stretching vibration than the Schiff base, confirming the structure of synthesized resin. A shift of absorption maxima towards longer wavelength within 10 to 34nm perceived in the initial 3 bands of compound PMBMNPn in comparison with BMNPn. A significant elevation in for resin was seen as compared to Schiff base.