Application of energy-filtering TEM to the nanocrystallization process in amorphous Fe84Nb7B9 alloy

Hirata, Akihiko; Hirotsu, Yoshihiko

doi:10.1007/s10853-006-7807-x

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“…8 shows the TEM image and SAED pattern of Fe 76 Si 4 B 10 P 5 Mo 5 glassy alloy annealed at 823 K, confirming the α-Mn type phase again. Here, it should be noticed that α-Mn type phase, which is usually observed in Fe-M-B (M=Nb or Zr) amorphous alloys during crystallization process [20][21][22], can be also formed in this FeSiBPMo glassy alloy system. With the annealing temperature increasing, it is found that α-Fe phase precipitates after annealing at temperature of 873 K (which is higher than that of Fig.…”

Section: Resultsmentioning

confidence: 97%