2021
DOI: 10.3390/foods10040807
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Application of NMR and Chemometrics for the Profiling and Classification of Ale and Lager American Craft Beer

Abstract: In this paper, Nuclear Magnetic Resonance spectroscopy (NMR)-based metabolomics were applied for the discrimination of ale and lager craft American beers. A modified pulse sequence that allows the efficient suppression of the water and ethanol peaks was used to achieve high-quality spectra with minimal sample preparation. The initial chemometrics analysis generated models of low predictive power, indicating the high variability in the groups. Due to this variability, we tested the effect of various data pretre… Show more

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Cited by 11 publications
(3 citation statements)
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“…Whereas, the highly responsive region near around 3.5 ppm represents the organic acids like citric acid, succinic acid, pyruvic, and acetic acid in both the samples 52 . Moreover, dextrins and sugars were observed at 5 ppm in the spectrum 53 . Overall, similar peaks patterns were observed in both the black and white wheat beer along with the reported literature 30 , 52 .…”
Section: Resultsmentioning
confidence: 98%
“…Whereas, the highly responsive region near around 3.5 ppm represents the organic acids like citric acid, succinic acid, pyruvic, and acetic acid in both the samples 52 . Moreover, dextrins and sugars were observed at 5 ppm in the spectrum 53 . Overall, similar peaks patterns were observed in both the black and white wheat beer along with the reported literature 30 , 52 .…”
Section: Resultsmentioning
confidence: 98%
“…Through innovative use of chemometrics that utilises peak-by-peak processing which systematically calculates interval-specific signals, they were able to show discrimination according to type and in some cases according to style (IPA vs ale beer) within the same class of top-fermented beers. Other attempts for the discrimination of ale and lager beers were also demonstrated by Vasas et al (2021). Although the sample size of some of the studies is generally small, the combination of a simpler analytical problem and a sophisticated technique (UHPLC-HRMS, GC-MS, or 1 H-NMR) indicates that discrimination of beer type is quite established at this point.…”
Section: According To the Type And Brewing Processmentioning
confidence: 98%
“…Thus, the overall aim of the present study was threefold: To investigate the possibility of generating molecular networks, to identify different indoles in beer and confirm their presence using NMR spectroscopy [17,25], and to analyze the sizes of the different colloidal fractions of beer samples using AF4 coupled to MALS.…”
Section: Introductionmentioning
confidence: 99%