1965
DOI: 10.1002/ange.19650770520
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Methods in Carbohydrate Chemistry. Herausgeg. v. R. L. Whistler, R. J. Smith, J. N. BeMiller und M. L. Wolfrom. Vol. IV: Starch. Academic Press, New York‐London 1964. 1. Aufl., XVI, 335 S., zahlr. Abb. u. Tab., geb. $ 13.50.

Abstract: Eine einfache Darstellungsmethode fur Chromoxydtrichlorid fanden R . B. Johannesen und H.-L. KrauJ. CrOC13 entsteht nach in siedendem BCl3 (+ 13 "C) bei gleichzeitigem Durchleiten von Stickstoff. Aus dem Reaktionsgemisch werden BC13 und restliches CrOzC12 durch Hochvakuumdestillation abgetrennt, anschlieoend sublimiert man CrOC13 an einen Kuhlfinger (-30 "C). So konnte eine homoopolare Cr(V)-Verbindung erstmals in guter Ausbeute (2 g = 50 %) gewonnen werden. / Chem. Ber. 97, 2094Ber. 97, (1964 / -Gn.[Rd 1651… Show more

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Cited by 7 publications
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“…Starches from unripe apples showed a low retrogradation susceptibility, as determined by two methods. The first method is based on the loss of the ability of starch polymers to form a complex with iodine [51]. The second method relates to the increase in the starch retrogradation (recrystallization) enthalpy ∆H r of the paste stored for a certain period of time during the heating in a differential scanning calorimeter (DSC).…”
Section: Retrogradationmentioning
confidence: 99%
See 1 more Smart Citation
“…Starches from unripe apples showed a low retrogradation susceptibility, as determined by two methods. The first method is based on the loss of the ability of starch polymers to form a complex with iodine [51]. The second method relates to the increase in the starch retrogradation (recrystallization) enthalpy ∆H r of the paste stored for a certain period of time during the heating in a differential scanning calorimeter (DSC).…”
Section: Retrogradationmentioning
confidence: 99%
“…The degree of retrogradation of the 1% water solution at 20, 8, and −20 • C was calculated using the below equation. The Whistler method [51] is based on the absorbance of the iodine-starch complex formed by amylose from a supernatant after centrifugation at point zero and also after 24, 48, and 72 h of storage. Spectrophotometric measurements were carried out in a spectrophotometer (Helios Gamma, 100-240, Runcorn, UK) at 635 nm.…”
Section: Degree Of Retrogradationmentioning
confidence: 99%