Ball milling assisted hydrothermal synthesis of ZrO2 nanopowders

Enhancing Dispersion of Yttria-Stabilized Tetragonal Zirconia Nanopowders with Microwave Solvothermal Synthesis

“…In addition, the particle size can be controlled in a narrow distribution range by changing hydrothermal synthesis conditions. For example, Reddy et al [18] reported that pure tetragonal ZrO2 nanoparticles were synthesized by hydrothermal method at 200 ℃ for 12 h. Duran et al [2] indicated that m-ZrO2 nanoparticles were prepared using a ball-milling-assisted hydrothermal technique in a temperature range of 125-200 °C and a time range of 1 min-15 h. These works all reveal the fact that the synthesis time decreased with increasing synthesis temperature. Besides, Gonzalo et al [19] also reported the formation of m-ZrO2 nanocrystals under subcritical hydrothermal conditions.…”

“…Zirconia (ZrO2) has received extensive attention due to its good physical and chemical properties, such as high mechanical strength, low thermal conductivity, desirable chemical stability, and excellent corrosion resistance. Based on these superior properties, zirconia nanopowder with excellent dispersion has been widely used to prepare high-performance structural and functional materials [1][2][3][4][5][6][7]. However, serious agglomeration phenomenon is often detected in ZrO2 nanoparticles synthesized by ordinary methods, such as co-precipitation [8], combustion synthesis [9], and sol-gel process [10,11], which possess high reaction temperature or high calcination temperature [12,13].…”

Synthesis and luminescent properties of ZrO2 and Dy3+-activated ZrO2 powders

“…ion irradiation and also calculated the TL kinetic parameters. Duran et al [16] have synthesized ZrO 2 nanopowder using ball milling assisted hydrothermal method and monoclinic crystal structure is obtained. Tamrakar et al [17] have synthesis ZrO 2 :Eu 3?…”