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1968
1968
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“…The liberated alkyl iodide was oxidized to HI03 and determined iodometrically. Pietrogrande, Bordin, and Fini (237) obtained correct methoxyl values on substances yielding low values by the Zeisel method by employing a methylimide apparatus and decomposing the sample with a mixture of hydriodic acid and ammonium iodide. Shah, Gobeille, and Mowery (270) modified the apparatus and procedure of Steyermark for micromethoxyl determination.…”
mentioning
confidence: 99%
“…The liberated alkyl iodide was oxidized to HI03 and determined iodometrically. Pietrogrande, Bordin, and Fini (237) obtained correct methoxyl values on substances yielding low values by the Zeisel method by employing a methylimide apparatus and decomposing the sample with a mixture of hydriodic acid and ammonium iodide. Shah, Gobeille, and Mowery (270) modified the apparatus and procedure of Steyermark for micromethoxyl determination.…”
mentioning
confidence: 99%
“…The titrant was barium acetate solution; alkali metals and halides did not interfere. Pietrogrande and Fini(236) investigated the possibility of reducing the sample weight in closed flask combustions. The reduction was effected without any essential modifications.…”
mentioning
confidence: 99%
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