“…Figure b showed the C 1s high-resolution XPS spectrum of CF@BOC-15 whose curves were fitted with CC (284.5 eV), C–O (285.9 eV), and CO (287.9 eV), distinguishing the indeterminate carbon in the C 1s spectrum of CF@Bi 2 O 3 (Figure S3b) shown as C–C (284.8 eV), C–O–C (285.8 eV), and O–CO (288.5 eV) . The two strong peaks in the Bi 4f spectrum of CF@Bi 2 O 3 (Figure S3c) at 159.0 and 164.3 eV could be attributed to Bi 4f 7/2 and Bi 4f 5/2 , , revealing the positive trivalent oxidation state of bismuth. As for Bi 4f of CF@BOC-15 (Figure c), the peaks at 159.0/164.3 and 159.5/164.8 eV could be attributed to Bi 3+ in Bi 2 O 3 and Bi 2 O 2 CO 3 , respectively. ,, As for the O 1s (Figure d), four peaks concentrated at 530.1, 531.1, 521.9, and 533.2 eV were attributed to Bi–O in Bi 2 O 2 CO 3 , CO 3 2– , and Bi–O–Bi in Bi 2 O 3 , and absorbed water, respectively. − In addition, the O 1s spectra in Figure S3d also showed two types of peaks (529.7 and 531.0 eV). , The former corresponded to Bi–O–Bi in Bi 2 O 3 , while the latter was identified as a surface hydroxyl group.…”