“…The XRD patterns of the HNT-DMA and HNT-DMA-PPy@Ag nanocomposites are shown in Figure 5 b. One can note the presence of reflection peak situated at 11.9°, corresponding to the basal distance of the HNT clay d(001), moreover the presence of diffraction peaks at 19.9°, 24.5°, 35.1°, 38.3°, 54.6°, and 62.4° which confirm that the crystalline structure of HNT clay is well maintained in all samples [ 29 ], after pretreatment and upon photopolymerization ( Figure 5 b) The presence of diffraction peaks at 38.2°, 44.4°, 64.4°, and 77.39° are corresponding to the (111), (200), (220), and (311) diffraction planes of Ag, respectively [ 30 ]. These patterns confirm metallic nature of Ag nanoparticles, resulted upon the photopolymerization of Py in the presence of AgNO 3 [ 11 ], The AgNPs average size was equal 82 nm, the latter was estimated from the full width half maximum (FWHM) of the highest intensity (111) peak of Ag.…”