“…From the scanning electron micrographs, we can see that breakage changed the morphology of particles: primary particles on agglomerate surfaces were broken and particle surfaces became very rough, especially for WL13 and WL11. These changes decreased the particle size [D 3,2 decreased 4.8% (P = 0.023), 4.6% (P = 0.01), 12.4% (P = 0.01), and 23.8% (P = 0.000) for WL10, WL31, WL11, and WL13, respectively] and increased the SSA [SSA increased 5.1% (P = 0.027), 9.1% (P = 0.000), 16.4% (P = 0.01), and 31.2% (P = 0.000) for WL10, WL31, WL11, and WL13, respectively] and particle density [particle density increased 19.5% (P = 0.002), 20.0% (P = 0.001), 22.0% (P = 0.001), and 11.7% (P = 0.001) for WL10, WL31, WL11, and WL13, respectively], which is consistent with previous research (Boiarkina et al, 2016;Han et al, 2020;Hazlett et al, 2020;Zhang et al, 2020). Also, the larger the particles, the greater the changes that occurred.…”