Bridging colloidal and electrochemical syntheses of metal nanocrystals with seeded electrodeposition for tracking single nanocrystal growth

Verma, Ekta; Choi, Myung-Hoon; Kar, Nabojit; Baker, Lane A.; Skrabalak, Sara E.

doi:10.1039/d4nr00202d

Nanoscale

2024

DOI: 10.1039/d4nr00202d

|View full text |Cite

Bridging colloidal and electrochemical syntheses of metal nanocrystals with seeded electrodeposition for tracking single nanocrystal growth

Ekta Verma,

Myung-Hoon Choi,

Nabojit Kar

et al.

Abstract: Metal nanocrystals (NCs) produced by colloidal synthesis have a variety of structural features, such as different planes, edges, and defects. Even from the best colloidal syntheses, these characteristics are distributed...

Help me understand this report

Search citation statements

Order By: Relevance

Paper Sections

Select...

Citation Types

Supporting

Mentioning

Contrasting

Year Published

2024

Publication Types

Select...

Article4

Relationship

Self Cite0

Independent4

Authors

Journals

Cited by 4 publications

References 55 publications

Supporting

Mentioning

Contrasting

Order By: Relevance

An overview of In2S3 and In2S3-based photocatalyst: characteristics, synthesis, modifications, design strategies, and catalytic environmental application

Mishra,

Gadore,

Ahmaruzzaman

2024

Journal of Environmental Chemical Engineering

View full text Add to dashboard Cite

An overview of In2S3 and In2S3-based photocatalyst: characteristics, synthesis, modifications, design strategies, and catalytic environmental application

Mishra,

Gadore,

Ahmaruzzaman

2024

Journal of Environmental Chemical Engineering

View full text Add to dashboard Cite

Optically Transparent Carbon Electrodes for Single Entity Electrochemistry

Vernon,

Pungsrisai,

Wahab

et al. 2024

ACS Electrochem.

View full text Add to dashboard Cite

We demonstrate the application and benefit of optically transparent carbon electrodes (OTCEs) for single entity nanoelectrochemistry. OTCEs are prepared by pyrolyzing thin photoresist films on fused quartz coverslips to create conductive, transparent, thin films. Optical, electrical, topographical, and electrochemical properties of OTCEs are characterized to evaluate their suitability for single entity electrochemistry. Nanoscale electrochemical imaging of the OTCEs using scanning electrochemical cell microscopy (SECCM) revealed uniform electrochemical activity for reduction of the hexaammineruthenium(III) redox complex, that was comparable to Au-coated glass, and in contrast to the heterogeneity observed with commonly used indium tin oxide (ITO) substrates. Additionally, we demonstrate the utility of the prepared OTCEs for correlative SECCM�scanning electron microscopy studies of the hydrogen evolution reaction at the surface of Au nanocubes. Lastly, we demonstrate the benefit of OTCEs for optoelectrochemical experiments by optically monitoring the electrodissolution of Au nanocrystals. These results establish OTCE as a viable transparent support electrode for multimode electrochemical and optical microscopy of nanocrystals and other entities.

show abstract

Electrochemical deposition of gold nanoparticles on carbon ultramicroelectrode arrays

Weber,

Strom,

Simoska

2024

Nanoscale

View full text Add to dashboard Cite

show abstract

scite is a Brooklyn-based organization that helps researchers better discover and understand research articles through Smart Citations–citations that display the context of the citation and describe whether the article provides supporting or contrasting evidence. scite is used by students and researchers from around the world and is funded in part by the National Science Foundation and the National Institute on Drug Abuse of the National Institutes of Health.

Contact Info

customersupport@researchsolutions.com

10624 S. Eastern Ave., Ste. A-614

Henderson, NV 89052, USA

This site is protected by reCAPTCHA and the Google Privacy Policy and Terms of Service apply.

Blog Terms and Conditions API Terms Privacy Policy Contact Cookie Preferences Do Not Sell or Share My Personal Information

Made with 💙 for researchers

Part of the Research Solutions Family.

Bridging colloidal and electrochemical syntheses of metal nanocrystals with seeded electrodeposition for tracking single nanocrystal growth

Abstract: Metal nanocrystals (NCs) produced by colloidal synthesis have a variety of structural features, such as different planes, edges, and defects. Even from the best colloidal syntheses, these characteristics are distributed...

Cited by 4 publications

References 55 publications

An overview of In2S3 and In2S3-based photocatalyst: characteristics, synthesis, modifications, design strategies, and catalytic environmental application

An overview of In2S3 and In2S3-based photocatalyst: characteristics, synthesis, modifications, design strategies, and catalytic environmental application

Optically Transparent Carbon Electrodes for Single Entity Electrochemistry

Electrochemical deposition of gold nanoparticles on carbon ultramicroelectrode arrays

Contact Info

Product

Resources

About