1979
DOI: 10.1021/ac50043a026
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Calibration of an inductively coupled plasma-atomic emission spectrometer for the analysis of environmental materials

Abstract: 0b°Values as high as 4800 have been reported by others (15, 16). 6 Values as high as 700 have been reported by others (15, 16).regarding the validity of the reported results; they can only be considered as qualitatively suggestive of accuracy. SUMMARYThe present results have shown that fluoride compounds are fairly rapidly converted to CaF2 in the arc in the presence of excess calcium, that complete vaporization of the CaF2

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Cited by 114 publications
(38 citation statements)
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“…The leaf litter, twigs, branches and fruits were then ground into powder using a tungsten carbide vibrating mixer mill (Mitamura, Retch 18-34) and digested with nitric acid in a high pressure Teflon Vessel (Quaker et al, 1970;Koyama and Sutoh, 1987). The concentrations of elements, Ca, Mg, AI, Fe, Sand P, were determined by an Inductive Coupled Plasma Atomic Emission Spectrometer (lCPS-2000; Shimadzu, Japan).…”
Section: Laboratory Methods and Data Analysesmentioning
confidence: 99%
“…The leaf litter, twigs, branches and fruits were then ground into powder using a tungsten carbide vibrating mixer mill (Mitamura, Retch 18-34) and digested with nitric acid in a high pressure Teflon Vessel (Quaker et al, 1970;Koyama and Sutoh, 1987). The concentrations of elements, Ca, Mg, AI, Fe, Sand P, were determined by an Inductive Coupled Plasma Atomic Emission Spectrometer (lCPS-2000; Shimadzu, Japan).…”
Section: Laboratory Methods and Data Analysesmentioning
confidence: 99%
“…Some samples which could not be analyzed immediately were stored at 4"C after the addition of concentrated HCl adjusted to pH 1, except for chlorine determination. Analytical methods were as follows: Nitrate concentration was measured with an ultraviolet spectrometer (Wetter and Uglum 1970), chlorine ion by thiocyanate method (Adriano and Doner 1982), bicarbonate content by titrating with dilute sulfuric acid (Bower and Wilcox 1965), pH using a pH meter with a glass electrode, total elemental concentrations of AI, Fe, Si, Mn, Ca, Mg, and S were measured by inductively coupled plasma atomic emission spectrometry (ICP) using Simadzu ICPS-2000 (Quaker et al 1970), and K and Na concentrations were measured by atomic adsorption spectrometry, AAS (Dale and Norman 1982). Major elemental composition of soils and rocks samples was also analyzed by ICPS-2000 and AAS after digestion with hydrogen fluoride and hydrogen chloride in a closed Teflon vessel (Uchida 1979).…”
Section: Methodsmentioning
confidence: 99%
“…Samples were digested with HNO 3 in a high pressure Tefflon Vessel (Quaker et al, 1970;Koyama & Sutoh, 1987). After heating and digest in 160 °C for 5 hours and cooling overnight, then adding HF 10% and H 3 BO 3 4%.…”
Section: Sampling and Analysismentioning
confidence: 99%