CarbonCarbon Bond Formation

Tanaka, Kōichi

doi:10.1002/9783527626410.ch3

Solvent‐Free Organic Synthesis 2008

DOI: 10.1002/9783527626410.ch3

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CarbonCarbon Bond Formation

Kōichi Tanaka

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2018

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Molecular iodine as a mild catalyst for cross-coupling of alkenes and alcohols

Čebular

Stavber

2018

Pure and Applied Chemistry

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C-C bond formation is one of the most fundamental approaches toward molecular diversity in organic synthesis. In pursuit of environmentally friendlier chemical approaches to organic chemistry, we present a new metal-free method for direct dehydrative cross-coupling of alcohols and alkenes using molecular iodine as a Lewis acid catalyst under solvent-free reaction conditions. The reaction is atom-economical, tolerant to air and allows simple synthetic procedure, furnishing C sp 3 -C sp 2 coupling products with yields up to 97 %. The method has proved efficient for coupling of secondary benzyl alcohols with phenyl-substituted alkenes.

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Molecular iodine as a mild catalyst for cross-coupling of alkenes and alcohols

Čebular

Stavber

2018

Pure and Applied Chemistry

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show abstract

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CarbonCarbon Bond Formation

Cited by 1 publication

References 227 publications

Molecular iodine as a mild catalyst for cross-coupling of alkenes and alcohols

Molecular iodine as a mild catalyst for cross-coupling of alkenes and alcohols

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