Catalytic pyrolysis of 5-Amino-1H-Tetrazole with copper and its oxide: A deep insight into the combustion mechanism for high nitrogen compound

Zhou, Sanming; Chen, Jiu; Li, Xuan; Fan, Jia; Zhang, Dan; Xie, Lifeng; Li, Bin; Jiang, Lin

doi:10.1016/j.fuel.2022.126764

Fuel

2023

DOI: 10.1016/j.fuel.2022.126764

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Catalytic pyrolysis of 5-Amino-1H-Tetrazole with copper and its oxide: A deep insight into the combustion mechanism for high nitrogen compound

Sanming Zhou

Jiu Chen²,

Xuan Li³

et al.

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Cited by 9 publications

References 44 publications

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Analysis of thermal stability for slow burning propellant based on isothermal testing: Self‐accelerating decomposition temperature (SADT) calculation and validation

Luo,

Xia,

Wang

et al. 2024

Propellants Explo Pyrotec

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Burning rate suppressants (BRSs) refer to a series of additives that reduce the burning rate of propellants, crucial for achieving sustained and stable thrust. This research focuses on assessing the impact of ammonium sulfate and ammonium oxalate on thermal stability and their potential as BRSs. Due to the stronger inhibitory effect of ammonium sulfate on the AP proton transfer process, the activation energy of propellant's first decomposition can be increased from 94.71 kJ mol−1 to 129.69 kJ mol−1 at a 3 % addition level. Based on Semenov model, the self‐accelerated decomposition temperatures (TSADT) were calculated and validated through 7‐day isothermal test. Introducing ammonium sulfate and ammonium oxalate raised the TSADT from 197.31 °C to 220.90 °C and 215.06 °C, respectively, deviating less than 4 % from experimental results. Among the propellants tested, those with ammonium sulfate showed prolonged response delay times (44.43–33.60 h), lower superheating temperatures (222.8–445.5 °C), and reduced mass loss rates (33.0–71.4 %) after 7 days of isothermal storage at 220–240 °C. The consistency between thermal analysis and isothermal test underscores the significant impact of activation energy on thermal stability.

show abstract

Analysis of thermal stability for slow burning propellant based on isothermal testing: Self‐accelerating decomposition temperature (SADT) calculation and validation

Luo,

Xia,

Wang

et al. 2024

Propellants Explo Pyrotec

View full text Add to dashboard Cite

show abstract

Insights into pyrolysis and combustion mechanism of green energetic agent 5-amino-1 h-tetrazole with different particle sizes

Li,

Zhou,

Zhao

et al. 2024

J Therm Anal Calorim

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Pyrolysis kinetics and reaction mechanism studies of 5-Amino-1H-Tetrazole with thermogravimetry/ differential scanning calorimetry/ Fourier transform infrared analysis

Chen,

Zhou,

Jiang

et al. 2024

Journal of Analytical and Applied Pyrolysis

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Catalytic pyrolysis of 5-Amino-1H-Tetrazole with copper and its oxide: A deep insight into the combustion mechanism for high nitrogen compound

Cited by 9 publications

References 44 publications

Analysis of thermal stability for slow burning propellant based on isothermal testing: Self‐accelerating decomposition temperature (SADT) calculation and validation

Analysis of thermal stability for slow burning propellant based on isothermal testing: Self‐accelerating decomposition temperature (SADT) calculation and validation

Insights into pyrolysis and combustion mechanism of green energetic agent 5-amino-1 h-tetrazole with different particle sizes

Pyrolysis kinetics and reaction mechanism studies of 5-Amino-1H-Tetrazole with thermogravimetry/ differential scanning calorimetry/ Fourier transform infrared analysis

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