2022
DOI: 10.16984/saufenbilder.1124183
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Characterization of Cobalt Oxalate Dihydrate Obtained from Spent Co-Mo/Al2O3 Hydrodesulfurization Catalyst

Abstract: In this study, roasted spent Co-Mo/Al2O3 hydrodesulfurization (HDS) catalyst was dissolved in oxalic acid (H2C2O4) solution and optimum conditions were determined for obtaining cobalt oxalate dihydrate (CoC2O4∙2H2O). The thermal decomposition behavior of the obtained CoC2O4∙2H2O was investigated by TG/DTG-DTA analysis. The characterization of CoC2O4∙2H2O was carried out by XRD, FT-IR and SEM-EDS analytical techniques. Optimum conditions for the production of CoC2O4∙2H2O were determined as 25 oC temperature, 0.… Show more

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