2011
DOI: 10.4028/www.scientific.net/amr.194-196.781
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Characterization of Well-Dispersed CeO<sub>2</sub> Nanoparticles Prepared by a New Method of Reverse Microemulsion

Abstract: Well-dispersed CeO2 nanoparticles were successfully prepared in a simple system composed of sodium bis (2-ethylhexyl) sulfosuccinate (AOT)- octane-water (W/O) microemulsion in this paper. The morphology and microstructure of the products were characterized by the laser particle size analyzer, Fourier transform infrared spectroscopy (FT-IR), X-ray diffractometer (XRD), differential scanning calorimeter (DSC) and transmission electron microscope (TEM). It was found that the CeO2nanoparticles obtained from this m… Show more

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“…If the surfactant coating is present after drying of the particles, it can also reduce the aggregation during calcinations steps, leading to very small, disperse particles after heat treatment at up to 800°C. 147 On the contrary, even a combined application of peptizing surfactants and ultrasonic agitation after the precursor 130 Ce 2 (CO 3 ) 3 P/C 400-1000 20-50 J.-G. Li et al 123 Ce(NO 3 ) 3 P/C 300-1000 5-65 Arul et al 131 Ce(NH 4 ) 2 (NO 3 ) 6 P/C 600 5 Hassanzade-Tabrizi et al 124 CeCl 3 P/C 100-900 10-50 Suresh et al 128 Ce(NO 3 ) 3 P/C 450-900 10-50 Mohamed et al 132 Ce(NO 3 ) 3 MW 160/500 8-15 Liao et al 133 Ce(NH 4 ) 2 (NO 3 ) 6 MW $100 2 Chen and Chang 134 Ce(NO 3 ) 3 Sol 30-90 7-20 Li et al 125 CeCl 3 Sol 40 2-4 135 Shuk, Greenblatt et al [136][137][138][139][140][141][142] Ce(NO 3 ) 3 HT 260 10-50 Hirano et al 143 Ce(NH 4 ) 2 (NO 3 ) 6 HT 150-240 3-9 Hakuta et al 126 Ce(NO 3 ) 3 HT 250-400 20-250 Yin et al 144 Ce(NH 4 ) 2 (NO 3 ) 6 Sono 80 3-7 Yu et al 145 Ce(NH 4 ) 2 (NO 3 ) 6 Sono 80 3-7 Masui et al 146 Ce(NO 3 ) 3 ME RT 2-5 Feng et al 147 Ce(NO 3 ) 3 ME RT/800 25-50…”
Section: Water-based Chemical Methodsmentioning
confidence: 97%
“…If the surfactant coating is present after drying of the particles, it can also reduce the aggregation during calcinations steps, leading to very small, disperse particles after heat treatment at up to 800°C. 147 On the contrary, even a combined application of peptizing surfactants and ultrasonic agitation after the precursor 130 Ce 2 (CO 3 ) 3 P/C 400-1000 20-50 J.-G. Li et al 123 Ce(NO 3 ) 3 P/C 300-1000 5-65 Arul et al 131 Ce(NH 4 ) 2 (NO 3 ) 6 P/C 600 5 Hassanzade-Tabrizi et al 124 CeCl 3 P/C 100-900 10-50 Suresh et al 128 Ce(NO 3 ) 3 P/C 450-900 10-50 Mohamed et al 132 Ce(NO 3 ) 3 MW 160/500 8-15 Liao et al 133 Ce(NH 4 ) 2 (NO 3 ) 6 MW $100 2 Chen and Chang 134 Ce(NO 3 ) 3 Sol 30-90 7-20 Li et al 125 CeCl 3 Sol 40 2-4 135 Shuk, Greenblatt et al [136][137][138][139][140][141][142] Ce(NO 3 ) 3 HT 260 10-50 Hirano et al 143 Ce(NH 4 ) 2 (NO 3 ) 6 HT 150-240 3-9 Hakuta et al 126 Ce(NO 3 ) 3 HT 250-400 20-250 Yin et al 144 Ce(NH 4 ) 2 (NO 3 ) 6 Sono 80 3-7 Yu et al 145 Ce(NH 4 ) 2 (NO 3 ) 6 Sono 80 3-7 Masui et al 146 Ce(NO 3 ) 3 ME RT 2-5 Feng et al 147 Ce(NO 3 ) 3 ME RT/800 25-50…”
Section: Water-based Chemical Methodsmentioning
confidence: 97%