“…Solidphase microextraction (SPME) is a simple, sensitive, robust, reliable, low cost sampling technique based on analyte diffusion that combines the advantages of both static and dynamic headspace for qualitative volatile analysis [9]. It has been widely adopted for use in food flavour analysis and most especially in legumes [10,11]. The amount of an analyte sorbed on the SPME fibre and the resulting sensitivity are determined both by sorption kinetics and by the distribution coefficient of the compound between the fibre surface and the sample.…”