Specimen Handling, Preparation, and Treatments in Surface Characterization 2002
DOI: 10.1007/0-306-46913-8_7
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Chemical Modification of Surfaces

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“…It is essential to characterize the chemical state and structure of the working catalyst. This requires specialized instrumentation so these supported catalysts can be prepared under well-defined conditions (e.g., reduced in H 2 at a given temperature and pressure) and then transferred directly into UHV for surface analysis[20, 21]. Since supported nanoparticles in both metallic and sulfided states are highly reactive and will quickly oxidize when exposed even briefly to air at room temperature, special care must be taken to avoid any exposure to the atmosphere when the transfer into UHV is made[21].…”
Section: Surface Analysis and Industrial Catalysismentioning
confidence: 99%
“…It is essential to characterize the chemical state and structure of the working catalyst. This requires specialized instrumentation so these supported catalysts can be prepared under well-defined conditions (e.g., reduced in H 2 at a given temperature and pressure) and then transferred directly into UHV for surface analysis[20, 21]. Since supported nanoparticles in both metallic and sulfided states are highly reactive and will quickly oxidize when exposed even briefly to air at room temperature, special care must be taken to avoid any exposure to the atmosphere when the transfer into UHV is made[21].…”
Section: Surface Analysis and Industrial Catalysismentioning
confidence: 99%