2012
DOI: 10.1039/c2jm14906k
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Chemically enhanced thermal stability of anodized nanostructured zirconia membranes

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Cited by 6 publications
(3 citation statements)
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“…It has been reported that ZrO 2 NTs undergo significant morphological changes when heat-treated at temperatures >600 °C due to changes in their crystal structure, but retain their nanotubular structure at lower temperatures. 30,31 Therefore, the morphological stability, observed in this work at 600 °C, is in good agreement with prior literature. 30,31…”
Section: Morphological Characterizationsupporting
confidence: 91%
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“…It has been reported that ZrO 2 NTs undergo significant morphological changes when heat-treated at temperatures >600 °C due to changes in their crystal structure, but retain their nanotubular structure at lower temperatures. 30,31 Therefore, the morphological stability, observed in this work at 600 °C, is in good agreement with prior literature. 30,31…”
Section: Morphological Characterizationsupporting
confidence: 91%
“…30,31 Therefore, the morphological stability, observed in this work at 600 °C, is in good agreement with prior literature. 30,31…”
Section: Morphological Characterizationsupporting
confidence: 91%
“…Based on earlier reports, these nanotubes were then chemically treated with DI water and aqueous ammonia (Fig. 2(c-d)) to alter the chemical composition [11,12]. While DI water was meant for cleaning the anodized structure of residual electrolyte, the ammonia treatment helps neutralize [11] the halide ions that impair thermal stability.…”
Section: Resultsmentioning
confidence: 99%