ChemInform Abstract: Condensed Isoquinolines. Part 38. Azolo[b]isoquinolines from 2‐(Halomethyl)benzoic Acid Derivatives.

Ковтуненко, В. А.; Потиха, Л. М.; Sypchenko, V. V.; Dmukhovsky, A. I.; Shelepyuk, A. V.

doi:10.1002/chin.201221158

ChemInform

2012

DOI: 10.1002/chin.201221158

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ChemInform Abstract: Condensed Isoquinolines. Part 38. Azolo[b]isoquinolines from 2‐(Halomethyl)benzoic Acid Derivatives.

В. А. Ковтуненко

Л. М. Потиха

V. V. Sypchenko

et al.

Abstract: Reaction of 2‐halomethylbenzonitriles (I) or related benzoate (XI) with azoles affords quaternary azolium salts, which undergo a base‐promoted intramolecular acylation furnishing fused isoquinoline derivatives.

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Synthesis and fluorescence of triazoloazines derivatives

2019

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Êè¿âñüêèé íàö³îíàëüíèé óí³âåðñèòåò ³ìåí³ Òàðàñà Øåâ÷åíêà, Êè¿â, Óêðà¿íà Ç âèêîðèñòàííÿì íîâîãî ï³äõîäó, ÿêèé áàçóºòüñÿ íà öèêë³çàö³¿ ñîëåé 4H-1,2,4-òð³àçîë-4-àì³íó íà îñíîâ³ ìåòèë (E)-4-áðîìî-2-áóòåíîàòó òà ìåòèë 2-(áðîìîìåòèë)áåíçîàòó, ñèíòåçîâàíî çàì³ùåí³ â ïåð³-ïîëîaeåííÿõ àì³íî-ã³äðîêñèïîõ³äí³ [1,2,4]òð³àçîëîàçèí³â. Âñòàíîâëåíî, ùî ñïîëóêè º ÷óòëèâèìè äî çì³íè ïîëÿðíîãî îòî÷åííÿ ó ðîç÷èíàõ ³ õàðàêòåðèçóþòüñÿ ïîçèòèâíîþ ñîëüâàòîõðîì³ºþ ïðè çá³ëüøåíí³ ïîëÿðíîñò³ ðîç÷èííèêà. Ðîç÷èíè ñïîëóê ó ÄÌÑÎ ïðîÿâëÿþòü ³íòåíñèâíó áëàêèòíó ôëþîðåñöåíö³þ ( em =460-468 íì), ùî çàòóõàº ç ÷àñîì. Ïîêàçàíî, ùî âîäà ãàñèòü ôëþîðåñöåíö³þ 1-àì³íî[1,2,4]òð³àçîëî[1,5-b]³çîõ³íîë³í-1-³é-10-oëàòó â îðãàí³÷íèõ ðîç÷èííèêàõ. ²íòåíñèâí³ñòü ôëþîðåñöåíö³¿ 1-àì³íî-10-ã³äðîêñè-1H,5H,10H-[1,2,4]òð³àçîëî[1,5-b]³çîõ³íîë³í-4-³þ ç³ çá³ëüøåííÿì êîíöåíòðàö³¿ âîäè â ÄÌÑÎ â ìåaeàõ â³ä 0,05 äî 0,5% (v/v) çðîñòàº. Òîìó öÿ ñïîëóêà º âèñîêî÷óòëèâèì çîíäîì äëÿ êîíòðîëþ ñòóïåíÿ îñóøåííÿ äèìåòèëñóëüôîêñèäó.

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Synthesis and fluorescence of triazoloazines derivatives

2019

VKhKhT

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ChemInform Abstract: Condensed Isoquinolines. Part 38. Azolo[b]isoquinolines from 2‐(Halomethyl)benzoic Acid Derivatives.

Abstract: Reaction of 2‐halomethylbenzonitriles (I) or related benzoate (XI) with azoles affords quaternary azolium salts, which undergo a base‐promoted intramolecular acylation furnishing fused isoquinoline derivatives.

Cited by 1 publication

References 1 publication

Synthesis and fluorescence of triazoloazines derivatives

Synthesis and fluorescence of triazoloazines derivatives

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