ChemInform Abstract: COPPER‐CATALYZED ADDITIONS OF SULFONYL IODIDES TO SIMPLE AND CYCLIC ALKENES

LIU, L. K.; Jen, Kwan-Yue

doi:10.1002/chin.198021183

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2023

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“…Sodium sulfinates 2 were prepared according to the literature report. 18 All of the experiments were monitored by thin-layer chromatography (TLC) with UV light. The anode electrode and cathode electrode were graphite flakes (10 × 10 × 3 mm).…”

Section: ■ Experimental Sectionmentioning

confidence: 99%

Electrochemical Annulation of Indole-Tethered Alkynes Enabling Synthesis of Exocyclic Alkenyl Tetrahydrocarbazoles

Liu

et al. 2023

J. Org. Chem.

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An electrochemical sulfonylation-triggered cyclization reaction of indole-tethered terminal alkynes with sulfinates as sulfonyl sources has been developed, which affords exocyclic alkenyl tetrahydrocarbazoles in good chemical yields. This reaction features convenient operation and tolerates a wide scope of substrates with a variety of electronically and sterically diverse substituents. Furthermore, high E-stereoselectivity is observed for this reaction, which provides an efficient method for the preparation of functionalized tetrahydrocarbazole derivatives.

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Section: ■ Experimental Sectionmentioning

confidence: 99%

Electrochemical Annulation of Indole-Tethered Alkynes Enabling Synthesis of Exocyclic Alkenyl Tetrahydrocarbazoles

Liu

et al. 2023

J. Org. Chem.

View full text Add to dashboard Cite

show abstract

ChemInform Abstract: COPPER‐CATALYZED ADDITIONS OF SULFONYL IODIDES TO SIMPLE AND CYCLIC ALKENES

Abstract: Olefine (I) reagieren mit Arylsulfonyliodiden (II), im wesentlichen der Tosylverbindung, zu den Addukten (III).

Cited by 1 publication

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Electrochemical Annulation of Indole-Tethered Alkynes Enabling Synthesis of Exocyclic Alkenyl Tetrahydrocarbazoles

Electrochemical Annulation of Indole-Tethered Alkynes Enabling Synthesis of Exocyclic Alkenyl Tetrahydrocarbazoles

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