2000
DOI: 10.1002/chin.200040129
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ChemInform Abstract: Enantioselective Preparation and Enzymatic Cleavage of Spiroisoxazoline Amides.

Abstract: Enantioselective Preparation and Enzymatic Cleavage of Spiroisoxazoline Amides.-The synthesis of various spiroisoxazoline amides (XII)-(XV) using similar technologies is presented, involving an enantioselective high pressure Diels-Alder cycloaddition of spiroisoxazoline (I) with chiral compound (II), asymmetric dihydroxylation, and enantioselective retro-Diels-Alder reaction as key step. Amides (XII)-(XV) are tested for their ability to serve as a substrate for an isoxazoline-splitting enzyme isolated from the… Show more

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