Chemischer Informationsdienst
 1972
DOI: 10.1002/chin.197240283
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ChemInform Abstract: SYNTH. VON 3,5‐DIALKYL‐1,2,4‐TRITHIOLANEN, ZUORDNUNG DER KONFIGURATION UND KONFORMATIONSANALYSE DURCH PMR

S.B. Tjan1,
J. C. Haakman2,
C.J. Teunis3
et al.

Abstract: Durch Chlorierung der Disulfide (I), Umsetzung der über die Stufen (II) und (III) gebildeten Sulfenylchloride (IV) mit KJ zu den Disulfiden (V) und nachfolgende Cyclisierung mit Na‐sulfid werden die Dialkyl‐trithiolane (VI) dargestellt [Gesamtausbeuten 21‐57%].

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