ChemInform Abstract: SYNTHESE ORGANISCHER RHODANVERBINDUNGEN UEBERSICHT 45. MITT. TEIL 1, ALIPHATISCHE RHODANVERBINDUNGEN

Abstract

In dem ersten Teil der Übersicht werden Synthesen von aliphatischen Rhodan= Verbindungen, z.B. (III), durch Austausch von Halogen durch den Thiocyanatrest behandelt.

Ion-pair extraction of thiocyanate from plasma and its gas chromatographic determination using on-column alkylation

“…Potassium selenocyanate was obtained from Aldrich Chemical Co. Tributylsulfonium perchlorate was synthesized according to the method of Milligan and Minor (17). Butyl thiocyanate (IR 2154 cm"1, sharp) was prepared by the reaction of butyl bromide and potassium thiocyanate (18), and butyl isothiocyanate (IR 2094 cm"1, broad) was synthesized from n-butylamine and carbon disulfide (19). Ethyl acetate was from Burdick and Jackson Distilled-in-Glass.…”