ChemInform Abstract: TELOMERIZATION OF ISOPRENE WITH PHENOL CATALYZED BY BIS(DIBENZYLIDENEACETONE)PALLADIUM

Zakharkin, L. I.; Medvedkov, V. N.; Petrushkina, E. A.

doi:10.1002/chin.198313116

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2009

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“…As described for almost every telomerisation 1:1adducts of diene and nucleophile, in this case phenoxybutenes (3,4) and butenylphenols, e.g. (6), and a linear dimer of butadiene, 1,3,7-octatriene (7), are also formed as by-products. Smutny discovered this reaction while working on oligomerisations of butadiene.…”

Section: Introductionmentioning

confidence: 75%

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Multiphase telomerisation of butadiene with phenol: optimisation and scale-up in different reactor types

2009

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The telomerisation with phenol is an efficient way to convert the well accessible 1,3-butadiene into products of higher value. This article describes the optimisation of this reaction both on a laboratory scale using a novel multiphase semi-batch mode and in a loop reactor as an alternative concept for a continuous operation mode. The optimised parameters are applied in a miniplant offering an interesting salt-free route to octadienylphenols.

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Section: Introductionmentioning

confidence: 75%

“…into insecticides 6 or pheromones. 7 Tsuji et al 8 and Beller et al 9 found further syntheses of natural and aromatic compounds starting with phenoxyoctadiene.…”

Section: Introductionmentioning

confidence: 99%

Multiphase telomerisation of butadiene with phenol: optimisation and scale-up in different reactor types

2009

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ChemInform Abstract: TELOMERIZATION OF ISOPRENE WITH PHENOL CATALYZED BY BIS(DIBENZYLIDENEACETONE)PALLADIUM

Abstract: Die Telomerisierung des Isoprens (II) mit Phenol (III) in Gegenwart des Katalysators (I) liefert ein Gemisch aus sechs isomeren l‐Phenoxy‐dimethyl‐octadienen (IV)‐(IX).

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Multiphase telomerisation of butadiene with phenol: optimisation and scale-up in different reactor types

Multiphase telomerisation of butadiene with phenol: optimisation and scale-up in different reactor types

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