Abstract:Three‐phase crystallization (TPC) was applied to purify S‐methyl‐2‐chloropropionate (S‐M2CP) from liquid enantiomer mixtures with various initial concentrations. TPC combines melt crystallization and vaporization to produce the desired crystalline solid along with the vapor from the liquid feed via a series of three‐phase transformations. The three‐phase states during TPC were calculated in terms of the thermodynamic properties of M2CP. Basically, the liquid mixture was gradually transformed to the S‐M2CP crys… Show more
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