Chiral resolution of l- and d-alanine and a racemic macrocyclic nickel(II) complex: synthesis and crystal structures

Ou, Guang‐Chuan; Li, Zhi-Zhang; Zhang, Min; Yuan, Xian‐You

doi:10.1007/s11243-013-9782-9

Transition Met Chem

2013

DOI: 10.1007/s11243-013-9782-9

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Chiral resolution of l- and d-alanine and a racemic macrocyclic nickel(II) complex: synthesis and crystal structures

Guang‐Chuan Ou

Zhi-Zhang Li

Min Zhang

et al.

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Cited by 6 publications

References 25 publications

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Chiral Recognition of Racemic Proline based on Chiral Macrocyclic Nickel(II) Complex: Synthesis and Crystal Structures

Jia

Zeng

et al. 2018

Zeitschrift anorg allge chemie

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The reactions of dl-proline with chiral macrocyclic Ni II complex [Ni(SS-L)](ClO 4 ) 2 in acetonitrile/water gave a six-coordinate enantiomer formulated as [Ni(SS-L)(l-Pro)](ClO 4 ) 2 ·H 2 O (1). Another enantiomer of [Ni(RR-L)(d-Pro)](ClO 4 ) 2 ·H 2 O (2) was obtained when [Ni(RR-L)](ClO 4 ) 2 was used (L = 5,5,7,12,12,4,8,11tetraazacyclotetradecane, Pro = proline). Single-crystal X-ray diffraction analyses of complexes 1 and 2 revealed that the Ni II atom has a distorted octahedral coordination arrangement, being coordinated by Scheme 1. The sketch of [Ni(SS-L)] 2+ (left) and [Ni(RR-L)] 2+ (right).

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Chiral Recognition of Racemic Proline based on Chiral Macrocyclic Nickel(II) Complex: Synthesis and Crystal Structures

Jia

Zeng

et al. 2018

Zeitschrift anorg allge chemie

Self Cite

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3D molecular fragment descriptors for structure–property modeling: predicting the free energies for the complexation between antipodal guests and β-cyclodextrins

Соловьев

2017

J Incl Phenom Macrocycl Chem

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CO2 fixation by macrocyclic nickel(II) complexes: synthesis and structures of helical chains constructed via hydrogen bonds involving imidazole

Liu

Ding

et al. 2014

Transition Met Chem

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Chiral resolution of l- and d-alanine and a racemic macrocyclic nickel(II) complex: synthesis and crystal structures

Cited by 6 publications

References 25 publications

Chiral Recognition of Racemic Proline based on Chiral Macrocyclic Nickel(II) Complex: Synthesis and Crystal Structures

Chiral Recognition of Racemic Proline based on Chiral Macrocyclic Nickel(II) Complex: Synthesis and Crystal Structures

3D molecular fragment descriptors for structure–property modeling: predicting the free energies for the complexation between antipodal guests and β-cyclodextrins

CO2 fixation by macrocyclic nickel(II) complexes: synthesis and structures of helical chains constructed via hydrogen bonds involving imidazole

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