1975
DOI: 10.1007/bf00925793
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Cleavage of tetrahydrofuran by trimethyliodosilane

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Cited by 5 publications
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“…Changing the bromination reagent to elemental bromine significantly improved the yields (Table 1, entries 4 and 5) [36]. Diethyl ether proved to be important as a solvent, the change to THF led to a total decomposition – most probably due to ring-opening reactions with bromosilanes [37]. Further, we investigated the influence of the amount of bromine on the reaction and concluded that stoichiometric quantities entirely fulfill the demands of the bromination (Table 1, entries 7 and 8).…”
Section: Resultsmentioning
confidence: 99%
“…Changing the bromination reagent to elemental bromine significantly improved the yields (Table 1, entries 4 and 5) [36]. Diethyl ether proved to be important as a solvent, the change to THF led to a total decomposition – most probably due to ring-opening reactions with bromosilanes [37]. Further, we investigated the influence of the amount of bromine on the reaction and concluded that stoichiometric quantities entirely fulfill the demands of the bromination (Table 1, entries 7 and 8).…”
Section: Resultsmentioning
confidence: 99%