2021
DOI: 10.1016/j.ica.2020.120215
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Cobalt complexes of an OSNSO-tetrapodal pentadentate ligand: Synthesis, structures and reactivity

Abstract: The novel pentadentate tetrapodal proligand 2,6-bis [(2-hydroxyphenyl)sulfanylmethyl]pyridine (1•H2) and its cobalt(II) complex [Co(1)] (2) were synthesized and characterized by several analytical (EA, ESI-MS) and spectroscopic methods (NMR or EPR, FT-IR), including X-ray crystallography for 1•H2. Cyclic voltammetry studies showed that 2 undergoes a reversible metal-based oxidation (Co II /Co III ). Complex 2 was designed to be applied to organometallic mediated radical polymerization (OMRP), however it exhibi… Show more

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