“…Previously, Fogagnolo et al [39] reported the compressibility of a similar system in the range of 200-500 MPa (the latter stage of compaction). By applying the Panelli and Ambrosio Filho equation [40] they showed that the green density decreases with AlN addition.…”
“…Previously, Fogagnolo et al [39] reported the compressibility of a similar system in the range of 200-500 MPa (the latter stage of compaction). By applying the Panelli and Ambrosio Filho equation [40] they showed that the green density decreases with AlN addition.…”
“…For instance, Fogagnolo et al [18] reported the effect of mechanical milling on morphology of powders. They related compaction behavior of powders to the microstructural evolutions occurred during milling and applied Panelli-Ambrosio Filho equation [19].…”
“…4). The reason is not completely clear; however, given the abundant evidence revealed from experiments [9][10][11][12][13][14][15] as well as simulations [16][17][18], it is now generally acknowledged that the change of slopes corresponds to a change in the dominate deformation mechanisms with decreasing grain size. In coarse-grained metals plastic deformation is governed by dislocation-mediated processes (nucleation, multiplication, motion and interaction etc.…”
Section: Dependence Of Hardness On Grain Size For Annealed Specimensmentioning
confidence: 99%
“…The reverse Hall−Petch behaviour observed at the finest nanoscale grain sizes is complicated and still in debate. It has been revealed by simulations [17,18] that the strength of NC Cu decreases with decreasing grain size in the grain size range of 3.28 to 6.56 nm, where the NC Cu deforms via a large number of small "sliding" events of atomic planes at grain boundaries, with only a minor part being caused by dislocation activity in grains. The reason for this softening at small grain sizes is due to a large fraction of atoms at grain boundaries.…”
Section: Annealing-induced Increase Of Hardness and Elastic Modulus O...mentioning
The evolution of the microstructure and mechanical properties of electrodeposited nanocrystalline Ni with different annealing procedures was studied systematically. For the annealed specimens hardness decreases with increasing average grain size but the dependence changes at different grain size ranges. The specimens annealed at a low temperature show higher hardness compared to the as-deposited nanocrystalline Ni, despite an increased measured average grain size. In association with this hardening an increase in elastic modulus and a decrease in microstrain was observed after annealing. With increasing annealing temperature both the tensile strength and the fracture strain were observed to decrease, this is companied with a transition from ductile to brittle in the fracture surfaces. These results indicated that the mechanical behaviour of nanocrystalline Ni depends not only on the average grain size but also on the grain boundary structure. A change in the grain boundary state arising from annealing may be responsible for the observed increase in hardness and elastic modulus as well as the deterioration of tensile properties.
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