2022
DOI: 10.1002/star.202100294
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Comparative Study of Heat‐Moisture Treatment and Annealing on Morphology, Crystallinity, Pasting, and Thermal Properties of Sohphlang (Flemingia vestita) Starch

Abstract: The impact of heat-moisture treatment (HMT) and annealing (ANN) on morphology, crystallinity, pasting, and thermal properties of sohphlang starch are determined. Heating of starch with 20%, 25%, and 30% moisture at 100 °C for 16 h is done for HMT while ANN is done for 24 h using 70%, 75%, and 80% moisture levels at 50 °C. Both HMT and ANN result in a rough surface structure and decreased birefringence at the center. The 1047/1022 ratio and crystallinity increase on modification but the A-type polymorph remains… Show more

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Cited by 9 publications
(9 citation statements)
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“…The results were consistent with the findings shown in Figure 2, also confirming that the rearrangement of starch chains may form a more compact crystalline structure, which requires higher energy for gelatinization. In addition, the reduction of the gelatinization temperature range (T c -T o ) implied that annealing can promote the formation of homogeneous microcrystalline and crystalline stability [28,37]. Under a total annealing time of 96 h, cycle numbers generally did not affect the gelatinization transition significantly, which was in line with studies on sweet potato starch under cycled annealing conditions [38].…”
Section: Thermal Propertiessupporting
confidence: 82%
See 1 more Smart Citation
“…The results were consistent with the findings shown in Figure 2, also confirming that the rearrangement of starch chains may form a more compact crystalline structure, which requires higher energy for gelatinization. In addition, the reduction of the gelatinization temperature range (T c -T o ) implied that annealing can promote the formation of homogeneous microcrystalline and crystalline stability [28,37]. Under a total annealing time of 96 h, cycle numbers generally did not affect the gelatinization transition significantly, which was in line with studies on sweet potato starch under cycled annealing conditions [38].…”
Section: Thermal Propertiessupporting
confidence: 82%
“…X-ray diffraction is used to observe the long-range order associated with the packing of double helices into ordered crystalline structures of starch [28]. The results of the X-ray pattern of native, annealed, and cycle-annealed water caltrop starch are shown in Figure 2.…”
Section: Crystalline Propertiesmentioning
confidence: 99%
“…As the time and temperature increased, the breakdown of annealed rice flour decreased gradually, and the final viscosity showed an increasing trend. The reduction in the pasting viscosity probably explains the difference in damage extent to the granules [38]. More damaged starch in annealed rice flour reduced the resistance to swelling.…”
Section: Pasting Properties Of Annealed Rice Kernels and Annealed Ric...mentioning
confidence: 99%
“…Annealed rice flour showed different results compared with annealed rice kernels. Annealed rice flour exhibited lower pasting properties than annealed rice kernels, which could be attributed to the interaction between protein and starch in rice, which restricts the swelling of rice starch granules during pasting by further crosslinking, thus reducing the pasting viscosity [38]. During annealing, protein in rice flour was exposed to water and heat more than in rice kernels, and there could be more significant interactions between protein and starch.…”
Section: Pasting Properties Of Annealed Rice Kernels and Annealed Ric...mentioning
confidence: 99%
“…• There were holes, cracks, and the more compact the amorphous portion of the starch granules [52] HMT (90,100,110,120 • C, 20 min) Sweet potato flour…”
Section: Tartary Buckwheat Starch (Tbs)mentioning
confidence: 99%