In recent decades, powder metallurgy technology has advanced considerably and been used to manufacture sintered structural components with extremely high dimensional accuracy and excellent surface finish. This process is based on the compression of a mixture of metal powder and sintering in an oven using controlled temperature and atmosphere. This technology meets copper alloys design with excellent mechanical properties at the lowest cost. This prompted us to study the effect of sintering temperature and aluminum concentration on the hardness, microstructure, and density of copper-aluminum (Cu-Al) alloys prepared by using the powder compaction process. In this work, samples of Cu-Al alloy with 5, 11, 14, and 18 wt. % of Al were prepared by mechanical alloying of elemental powders, followed by consolidation under a pressure of 12.5 MPa and sintering at 700-1000 C in vacuum for 90 min. Microstructural constituents were examined using X-ray diffraction. Density and hardness were measured and their changes with the size of the granules and the formed phases were studied. The 2 phase samples showed higher hardness.